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Article
Publication date: 9 April 2018

Syahrir Ridha, Afif Izwan Abd Hamid and Che Ku Afiza Hanim Che Ku Mazuan

The purpose of this paper is to investigate the mechanical properties changing of geopolymer cement under different brine salinity.

Abstract

Purpose

The purpose of this paper is to investigate the mechanical properties changing of geopolymer cement under different brine salinity.

Design/methodology/approach

Geopolymer Cement of Class F Fly Ash and Class G Cement slurries were prepared according to API RP 10B. The optimum alkaline activator/cement and water/cement ratio of 0.44 was used for geopolymer and Class G cement samples, respectively. The alkaline activator was prepared by mixing the proportion of Sodium Hydroxide (NaOH) solutions of 8 M and Sodium Silicate (Na2SiO3) using ratio of 1:2.5 by weight. The slurries were cured for 24 hours at 130oC and 3,000 psi in HPHT Curing Chamber followed by coring process. Both cement sample were immersed in brine water salinity up to 28 days with different brine salinity up to 30 per cent of NaCl. The mechanical properties were investigated using OYO Sonic Viewer-SX and Uniaxial Compressive Strength. The surfaces of the cement samples were extracted for Scanning Electron Microscope (SEM) and EDS tests to evaluate the morphology and chemical compositions of the cured samples.

Findings

The paper shows that geopolymer samples experiences strength reduction in brine water but the reduction rate of geopolymer is about half of the Ordinary Portland cement based oil well cement. The finding was also verified by SEM and EDS result.

Originality/value

This paper investigates the mechanical property changes of emerging geopolymer cement due to different water salinity. The results provide potential application of geopolymer cement for oil well cementing.

Details

International Journal of Structural Integrity, vol. 9 no. 2
Type: Research Article
ISSN: 1757-9864

Keywords

Article
Publication date: 1 October 2018

Syahrir Ridha, Afif Izwan Abd Hamid, Riau Andriana Setiawan and Ahmad Radzi Shahari

The purpose of this paper is to investigate the resistivity of geopolymer cement with nano-silica additive toward acid exposure for oil well cement application.

Abstract

Purpose

The purpose of this paper is to investigate the resistivity of geopolymer cement with nano-silica additive toward acid exposure for oil well cement application.

Design/methodology/approach

An experimental study was conducted to assess the acid resistance of fly ash-based geopolymer cement with nano-silica additive at a concentration of 0 and 1 wt.% to understand its effect on the strength and microstructural development. Geopolymer cement of Class C fly ash and API Class G cement were used. The alkaline activator was prepared by mixing the proportion of sodium hydroxide (NaOH) solutions of 8 M and sodium silicate (Na2SiO3) using ratio of 1:2.5 by weight. After casting, the specimens were subjected to elevated curing condition at 3,500 psi and 130°C for 24 h. Durability of cement samples was assessed by immersing them in 15 wt.% of hydrochloric acid and 15 wt.% sulfuric acid for a period of 14 days. Evaluation of its resistance in terms of compressive strength and microstructural behavior were carried out by using ELE ADR 3000 and SEM, respectively.

Findings

The paper shows that geopolymer cement with 1 wt.% addition of nano-silica were highly resistant to sulfuric and hydrochloric acid. The strength increase was contributed by the densification of the microstructure with the addition of nano-silica.

Originality/value

This paper investigates the mechanical property and microstructure behavior of emerging geopolymer cement due to hydrochloric and sulfuric acids exposure. The results provide potential application of fly ash-based geopolymer cement as oil well cementing.

Details

International Journal of Structural Integrity, vol. 9 no. 5
Type: Research Article
ISSN: 1757-9864

Keywords

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